Distillation Purpose: To conduct the distillation process‚ simple or fractional. Procedure: 1. Add 5ml of 20% ethanol: water mix to the distillation flask. 2. Add 23 stir bar 3. Make sure that the thermometer bulb is just below the Claisen Head‚ carefully. Be very gentle with the thermometers and take care not to break them. 4. Label 3 vials‚ 1‚2‚ and 3. 5. Place receiving vial 1 on ice to collect the distillate 6. Start the distillation by piling up hot sand around the distillation flask with
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The Extraction of Bio-ethanol from Apple (Malus domesticus) and Banana (Musa accuminata Colla) Peelings through the Process of Fermentation and Distillation Abstract Apple (Malus domesticus) and banana (Musa accuminata Colla) peelings are common household waste products. This study sought to extract bioethanol from these two peelings and to compare which sample can produce more bioethanol. About 400 grams of apple and banana peeling was obtained from the 1 kilogram bought from the supermarket
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Distillation of Alcoholic Beverages Pamela Mallari*‚ Symon Manuel‚ Katherine Merene and Charlene Mondelo Department of Chemistry‚ University of Santo Tomas‚ Manila‚ Philippines Abstract Distillation is a physical process used to separate chemicals from a mixture by the difference in how easily they vaporize. This experiment aims to (1) compare the efficiency of simple and fractional distillation‚ (2) distill and calculate the % of ethanol and (3) determine the % loss in distillation. Two
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Distillation of Alcohol Beverages Abstract Distillation is a process wherein a liquid is heated until its boiling point while the resultant hot vapors are subsequently captured and cooled‚ and the condensed vapors are collected. Among the many types of distillations‚ the fractional method or technique of distillation was used in this experiment. A step by step procedure was followed and an amount of 3.33 % of ethanol was obtained from the sample wine‚ Mateus Rose‚ which was used. Further
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Mona Vaidya 02/04/2014 CHE 317 Laboratory Experiment #1: Simple Distillation of Two Volatile Liquids Containing Non-Volatile Impurities Introduction: Simple distillation is a commonly used method to separate and purify the mixtures of organic liquids into their original components. Mixtures of two miscible liquids with two different boiling points were separated. Therefore‚ it can be said that the two organic compounds are separated by exploiting the different boiling temperatures of the liquids
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All about Distillation Distillation is a process that is used to purify a lot of substances on a domestic as well as commercial basis. It is very interesting to know about the process in detail as it is a natural process. The story begins when a liquid or solid state of mater responds to the heat in environment. The heat makes the liquid state or solid state of matter to convert into gas state. Liquid Gas (Vaporization) Solids
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then allowing toluene particles to separate in the later fractions when temperature is over 105 degrees Celsius. Lastly‚ it is concluded that fractional distillation is a more effective method as opposed to simple distillation because in fraction 7 of the simple‚ there was only around 36% toluene consumption versus a 96% in the fractional distillation. This is also due to the fact that using a fractionating column makes the samples more pure because it works better at separating the first couple of
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Chloroform‚ Acetone and Methanol) for sequential extraction. First of all plant materials were soaked in Hexane for 2-3 days with regular stirring. The mixture was then filtered by using Whatman No. 4 filter paper in to a glass beaker. 300ml of other solvent‚ Chloroform‚ was then added in the residue for 2-3 days. Similarly the mixture was filtered by using whatman No. 4 filter paper. After chloroform‚ Acetone and Methanol were added in residue for sequential extraction. Solvents; Hexane‚ Chloroform
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FRACTIONAL DISTILLATION *Ibale‚ I.‚ Ibanez‚ E.‚ Jao‚ E.‚ Joson‚ E.‚ Juanico‚ R. 2D Pharmacy‚ Faculty of Pharmacy‚ University of Santo Tomas Abstract Distillation is a commonly used method for separating mixtures based on differences in the conditions required to change the phase of components of the mixture. The product obtained by distillation is called the distillate. Volatility is the property of changing readily from a solid or liquid to a vapor. There are two types of distillation‚ simple
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f Fractional Distillation of a Solution Results 1. On a single graph‚ plot boiling point versus volume of distillate curves for the two distillations of the cyclohexane/toluene solutions (one from the simple distillation experiment and one from the fractional distillation experiment). The graph is to be computer generated and presentation quality (e.g.‚ appropriately scaled and labeled axes‚ descriptive title‚ and discernable data points). The data points are to be connected with a smooth
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