Recrystallization Experiment 2: Recrystallization & Melting Point • Most important method for the purification of organic solids • Separation of compounds based on differences in solubility between the compound of interest and its contaminants • Basic technique: 1. dissolve impure sample in an "appropriate" hot solvent Part A: Choosing a Solvent Part B: Purification of Phenacetin 2. cool solution slowly to induce crystal growth 3. filter resulting mixture to isolate crystals Reading:
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3 (Crystallization) Name: Parts A and B: 1. Please comment on the relative purity of your recrystallized salicylic acid (Hint: You should use your empirical data to support your claim). -The Salicylic acid that I obtained had a melting point range around 157-158 degrees Celsius for Part A. For Part B the melting point range was 156-157.5 degree Celsius. Part B‚ I would say the sample is less pure because of the notion that impurities lower the melting point. Since part A ‘s melting point
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3 3.4 Determination of Melting Point 3 4 Results and Calculation 4 4.1 Mass 4 4.2 Percent yield 4 4.3 Melting Point 4 4.4 Appearance 4 5 Discussion 5 6 Conclusion 5 References R1 Synopsis This report is based on preparation and recrystallization of aspirin. The objective of the experiment is to conduct the synthesis of aspirin and reinforce the skills of recrystallization and technique of melting point determination. Both experimental
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TBHQ/BHA/BHT - Maximum 200 gm/Ton of product d] Nitrogen : 10-12 % by volume of the fat‚ a nitrogencylinder With flowmeter is connected to suction of feed pump 40 3-5 Crystallization System ( Refrigeration Load : 1T/ HR-50 TR) Average Composition of a General purpose Bakery Fat : High Melting Point Middle Melting Point Lower Melting Point Til Oil (Sesame) 43-44ºC 35-36ºC 28-30ºC 50% 35% 12% 3% 100% Equipment Fat Temp ºC RPM Residence In Out Time Seconds Performer I 47+2 34+2 400-500 20 Performer
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the freezing point will be somewhat lower‚ and there will be a range of temperatures instead of a single temperature. PROBLEM To evaluate the samples‚ you will need a heating/cooling curve for pure Na2S2O35H2O that you can use as a standard. To create and use this curve‚ you must do the following. • Obtain a measured amount of pure Na2S2O35H2O. • Melt and freeze the sample‚ periodically recording the time and temperature. • Graph the data to determine the melting and freezing points of pure Na2S2O35H2O
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temperature Step 8: Cooled the solution in an ice bath for 5 minutes Step 9: Collected the crystalized solid by vacuum filtration Step 10: Measured the melting point for the crystalize solid Reagent Table: Table 1: The chemicals and properties used in the reaction Compound Quantity Molar Mass (g/mol) Melting Point (C) Boiling Point (C) Anthracene 0.5g 178.23 216-218 340 Maleic Anhydride 0.25g 98.06 54-56 200 Potassium Bromide 100 119 63.38 759 Xylene 6mL 106.17
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pleasant flavor‚ innocuousness‚ smoothness during application‚ adherence and easy intentional removal. This work involved the development of a lip balm formulated with certified organic raw materials and the execution of stability tests: fusion point determination‚ evaluation of organoleptic characteristics (color‚ odor and appearance) and functionality evaluation (spreadability test). The formulation selected after the Preliminary Stability Test was submitted to the Normal Stability Test under
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Organic chemistry 201 | Mixed Melting Points | Determination of an Unknown Solid | | [Type the author name] | 9/15/2011 | Purpose : The main purpose of this experiment was to identify an unknown compound/substance by performing multiple experimental melting point tests. Pure and impure solids were tested to see what affect pureness/impureness had on a melting point. Background: The melting point of a solid can be used to determine the purity of the solid. Pure samples usually have
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intermolecular attraction. For example‚ the freezing point of a solution is lower than that of the of the pure solvent and the boiling point is higher. Colligative properties of solution are those that depend on the concentration of solute particles in the solution‚ regardless of what kinds of particles are present the greater the concentration of any solute‚ the lower the freezing point and the higher the boiling point of a solution. FREEZING POINT LOWERING A liquid begins to freeze when temperature
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Exercise 1 Binary Solid-Liquid Diagram CHEM 112.1 – 2L Group 2 I. Data and Results Table 1.1 Break and arrest temperature of diphenylamine-naphthalene mixture. Table 1.1. Mole fraction of naphthalene‚ χB‚ and corresponding arrest and break temperature at each run. Run number | Mole Fraction‚XB | Ave. break temperature‚ ˚C | Ave. arrest temperature‚ ˚C | 1 | 1 | 72 | 35.4375 | 2 | 0.868388 | 72 | 35.4375 | 3 | 0.725218 | 62 | 35.4375 | 4 | 0.568895 | 49 | 35.4375
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