t-Pentyl Chloride is a compound that is created through an SN1 nucleophilic substitution reaction in addition with Hydrogen Chloride in order to isolate the product. A variety of procedural techniques were utilized during the experiment including extraction‚ washing liquids‚ drying liquids‚ gravity filtration‚ and simple distillation. When a single solute or compound is transferred between two different solutes‚ it is known as extraction. Another technique that was utilized was washing‚ in which
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Synthesis of t-Pentyl Chloride Introduction: Using SN1 reaction mechanism with hydrochloric acid‚ t-Pentyl alcohol was converted to t-Pentyl chloride in an acid catalyzed reaction. The reaction took place in a separatory funnel designed to separate immiscible liquids. The crude product was extracted by transferring a solute from one solvent to another. The process of washing the solutions by phase transfer was used in order to remove impurities from the main solvent layer. Finally‚ the crude
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Discussion/Conclusion In this experiment‚ t-pentyl chloride was synthesis by reacting concentrated hydrochloric acid using nucleophilic substitution sn1. In the substitution reaction the Hydrogen in HCl protonated the alcohol group in t-pentyl alcohol and turned it to a good leaving group (H2O). a tertiary carbon cation was formed. a nucleophilic attach of the negative Cl- attacked the carbon cation forming t-pentyl chloride [7]. As the reaction proceeded‚ extraction and distillation techniques
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Exp 23 B Synthesis of t-Pentyl Chloride 11-8-12 Purpose: The sysnthesis of t-Pentyl Chloride from alcohol. Procedure: Preparation of t-Pentyl Chloride. In a 125-mL separatory funnel‚ place 10.0 mL of t-pentyl alcohol (2-methyl-2-butanol‚ MW _ 88.2‚ d _ 0.805 g/mL) and 25 mL of concentrated hydrochloric acid (d _ 1.18 g/mL). Do not stopper the funnel. Gently swirl the mixture in the separatory funnel for about 1 minute. After this period of swirling‚ stopper the separatory funnel and
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Copper Chloride Lab Report Procedure Part A: 1. Pick up the container of copper chloride dehydrate‚ and observe material. Describe crystals in detail‚ and write down all of the observations. Part B: 1. Take a 100 ml beaker and fill ¼ of it with water. Use a spatula to add some copper chloride dehydrate to the beaker filled with water. Record the observations. Be sure to observe the water and the copper chloride dehydrate. 2. Stir the contents in the beaker with
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Purpose: The Purpose of this lab is to utilize‚ demonstrate and understand the various techniques and procedures used to gravimetric labs. For this particular lab we will utilize our scientific knowledge of related to gravimetric procedures to find the chloride content in an unknown soluble salt. Theory: Using our developed knowledge of the conservation of mass‚ solubility and precipitation it is possible (with some degree of error) to know the content of chlorine in a particular salt by dissolving
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From the experiment‚ it was determined that Sodium chloride had a crystalline structure‚ even after being broken into smaller pieces with a hammer. Even though there was two different types of Sodium chloride‚ coarse and fine‚ they still had a symmetrical‚ three-dimensional shape. All ionic compounds have this structure. It was also found that Sodium chloride had a high melting point and sugar had a low melting point. This is because Sodium chloride is ionic and the bonds holding it together take much
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energy lost by Calcium Chloride and gained by Ammonium Nitrate when dissolved in Water. Theory: Exothermic reactions are when net energy is lost in process of reaction. When solid calcium chloride (chemical formula CaCl₂) is placed in water‚ the calcium chloride dissolves and liberates heat in the process. Calcium chloride is one of the ingredients in instant "hot packs" sold in retail stores. Some concrete mixes incorporate calcium chloride to decrease drying time. Calcium chloride is also used as a
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The halides in unknown solution were identified as iodide and chloride based on their experimental E°(Ag/AgX) values‚ -0.16 ±0.01V and 0.22 ±0.02V respectively. These results were both accurate with percent error of 5.96% for iodine and 0.9% for chloride. The literature value of E°(Ag/AgI) and E°(Ag/AgCl) were -0.151V and 0.222V respectively (1). In addition‚ the literature vales lay within the 95% confidence interval for both halides therefore the results were accurate. These results were precise
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● Cobalt(II) Chloride Hexahydrate CoCl2.6H2O‚ was weighed in a weighing boat. The Cobalt(II) Chloride Hexahydrate was transferred into a 100mL volumetric flask dissolved in water. ● 25 mL of the dissolved was measured‚ using a graduated cylinder and few of the dissolved Cobalt (II) Chloride Hexahydrate‚ was poured into test tube. The test tube was labeled with a tape‚ to signify 25 mL and the spectrophotometer was used to record the U-V visible ABS (absorbance spectrum) with the wavelength of 515
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