Recrystallization and Melting Point Determination W. H. Bunnelle‚ L. A. Meyer‚ R. E. Glaser (Version 3) Introduction Consider what happens when a solid material is placed in a solvent in which it has a low solubility. Not much! A small fraction of the solid will dissolve‚ but the rest will just sit there. (Actually‚ it doesn’t just ’sit there’ since an equilibrium is in effect‚ with solid molecules going into solution‚ and an equivalent number of dissolved molecules reforming solid‚ but we
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References: Buchanan‚ G.W. "Solubility Tests and Recrystallization." CHEM 2203/2204 Organic Chemistry Laboratory Manual. By C.A. White. N.p.: n.p.‚ n.d. 21-31. Print. "IR Spectrum." Research Gate. N.p.‚ n.d. Web. 08 Oct. 2014. Wagner‚ Kathryn. "Like Dissolves Like." LIKE DISSOLVES LIKE (n.d.): n. pag. Web.
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Mabel M. Kimble September 21‚ 2014 Chemistry 234 Recrystallization of Benzoic Acid ABSTRACT The recrystallization of Benzoic Acid was performed to fully master the ability to purify a solid compound. This form of purification technique is especially important in chemical identification‚ where the melting point of the compound is taken to confirm its purity. In order to perform recrystallization a solubility test much be completed. Four solvents (95% Ethanol‚ Petroleum Ether‚ Acetone and distilled
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Introduction Recrystallization is a method used to purify solid organic compounds. Using the recrystallization technique‚ a solid compound is dissolved in a solvent and the compound slowly crystallizes as the solution cools. Using a filtration technique‚ a pure solid is produced when the molecules of the impure particles in the compound are excluded from the crystal lattice. After obtaining the pure compound‚ a melting point determination procedure can be done using a mel-temp device to correctly
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molecular weight is 151.2 g/mol. The melting point of pure compound is in the range of 169-172 ℃. During lab Paracetamol medication was dissolved in water‚ purified and recrystallized again. The purpose of the experiment was to learn basic recrystallization techniques that include hot and cold filtration. During experimental procedure sample was purified and its final melting point was measured. Procedure 1.0 g of impure Paracetamol was added to the flask with 2 boiling chips. 30 mL of distilled
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Recrystallization of Benzoic acid Chemistry 204-002 Date: 4/9/2011 Hector Ortega Recrystallization is a method used to purify compounds‚ and this is a very important procedure because compounds are naturally impure. Polarity and solubility play a big role in this experiment and these characteristics are exploited in order to have a crystallization of the desired compound. In this experimented benzoic acid was crystallize using ethanol and water. I chose these solvents based on part C of the experiment
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To: Aron Huckaba From: Peyton Lewis Date: 9/20/12 Subject: Experiment 3: “Identifying a Constituent of Panacetin” Partner: Julie Covington Introduction This experiment was a continuation of Experiment two‚ with a slightly different question to be answered. In this experiment‚ we are trying to find the identitiy of the unknown component of Panacetin. This is answering question 2 of the two questions that were to be answered in experiment 2. The equation of this reaction is as follows (and
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Objective: Separate and purify acetanilide from a mixture by recrystallization. Compare the melting points of crude and recrystallized acetanilide. Introduction : The most common method of purifying solid organic compounds is by recrystallization. In this technique‚ an impure solid compound is dissolved in a solvent and then allowed to slowly crystallize out as the solution cools. As the compound crystallizes from the solution‚ the molecules of the other compounds dissolved
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Separating the components of Panacetin Umar Hussaini Sneha Ray 9/30/14 Abstract In this lab we separated components of a simulated preparation‚ panacetin and making use of its acid base properties. To obtain such a pure compound‚ the compound we want must be separated from its other natural components‚ which can be done by manipulating physical and chemical properties. Panacetin contains sucrose‚ aspirin and an unknown which can be acetanilide or phenacetin in which phenacetin
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Experiment 1: Recrystallization – Evaluation Summary Last Name: Xavier First Name: Jessica Date: October 1st 2013 Lab Day/TA/Group: Wednesday(1:35pm)/Group A Labs reports must be typed and chemical structures must be drawn with ChemDraw. Report must not exceed three pages (including this page). Page limit does not include any attached spectra or references. ** Deductions for hand written report/structures and exceeding page limit ** Report Breakdown Data/Results: _________________
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