Bleach Oxidation of 9-Hydroxyfluorene The purpose of this experiment was to oxidize an alcohol (9-hydroxyfluorene) to a ketone (9-fluorenone) using aqueous sodium hypochlorite (bleach) as the oxidizing agent‚ while introducing techniques used in microscale experiments. Reaction: Results 1. Recrystallized Product Yield Product yield = (actual yield/theoretical yield) x 100% 3mL 9-hydroxyfluorene x (1mL/1000mL) x (0.09 mol/L) = 2.7 x 10-4 moles 0.05g 9-fluorenone / (180.20g/mol) = 2.77 x 10-4
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Oxidation of an Alcohol: Oxidizing Methoxybenzyl Alcohol to Methoxybenzaldehyde Using Phase-Transfer Catalysis PURPOSE OF THE EXPERIMENT Oxidize methoxybenzyl alcohol to methoxybenzaldehyde‚ using sodium hypochlorite as the oxidizing agent and tetrabutylammonium hydrogen sulfate as the phase-transfer catalyst. Monitor the progress of the reaction by thin-layer chromatography. BACKGROUND REQUIRED You should be familiar with extraction‚ evaporation‚ and thin-layer chromatography techniques
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April Goodson CHEM 242L-002 February 20‚ 2013 Oxidation of Cyclohexanone to Adipic Acid Abstract The cyclic ketone cyclohexanone was oxidized to adipic acid using the oxidizing agent nitric acid. The experiment yielded 0.2667 grams of adipic acid‚ giving a percent yield of 113.97%. Although the product was allowed to dry for one week‚ residual moisture was still present in the sample and a melting point could not be obtained. This error in the experiment either resulted from adding too much
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your hands are cleaned after every apple) 7. Start the timer and every ten minutes rate the progression of discolouration on each apple on the scale listed below. Take photos. 8. Repeat experiment (steps 1-7) one more time using the remaining apple. 9. Record the results in the table. SCALE 0 - no browning present 1- Brown dots 2 -Brown patches 3 - Half-covered light brown 4 - Completely light brown 5 - Completely dark brown Results: pH of Substance Time (mins) 0 10 20 30
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Acids & Bases: Reactions‚ Standardizations‚ & Titrations Experiments 21 & 22 Experimental Overview: The procedure for this experiment was carried out as instructed in the laboratory manual‚ Experiments in General Chemistry‚ 4th ed.‚ S.L. Murov‚ Experiment 21‚ Acids and Bases: Reactions and Standardizations‚ and Experiment 22‚ Acids and Bases: Analysis. There were modifications made by the instructor to dilute the 6M NaOH to 0.1M in 300mls
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Carboxylic acids are compounds which contain a carboxyl group‚ -COOH group‚ where the -COOH group is attached either to a hydrogen atom or to an alkyl group. One of the example of carboxylic acid is benzoic acid( benzene carboxylic acid) which has a benzene connected to the carboxyl carboxyl group‚ -COOH group. It has a formula of C6H5COOH. The carbon atom of a carboxyl group has a high oxidation state. Therefore‚ that many of the chemical reactions used for their preparation are oxidations. In this
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Lab Report: Acid and Base Indicator Lab The title of my lab report is “Acid and Base Indicator Lab” this lab is testing what household solutions area bases depending on what color they changed. You have to use the pH balance scale to determine Acid‚ Base‚ and Neutral. On this lab we used 7 different solutions to determine if it’s either base‚ acid‚ and neutral. These are ammonia‚ vinegar; drain cleaner‚ soft drink‚ baking soda‚ detergent‚ and lemon juice are the solutions that are going to be
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Lab Report Acids and Alkalis: Chemistry of Neutralization and Salt Formation Introduction: An acid is a group of chemicals. Acids are positively charged ions‚ they are liquid and are solutions of pure compounds in water. If you want to know if something is an acid‚ you can test it by using litmus paper. Acids will turn litmus paper red‚ whilst alkalis will turn it blue. Alkalis are negatively charged ions and are usually solid. Aim: To find out how much of different acids is needed to neutralize
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4 Strong Acid and Weak Base Lab PURPOSE: To find the molarity of an unknown acidic acid. MATERIALS: 1. 250 mL beaker 2. 10 mL graduated cylinder 3. 50 mL beaker 4. Funnel 5. 125 mL Erlenmeyer flask 6. 50 mL buret 7. Ring stand 8. Strong acid 9. Weak base 10. Phenolphthalein 11. De-ionized water. PROCEDURES: 1. Fill the buret with a weak base and place it in the ring stand. 2. Fill the 50 mL beaker with 30 mL of a strong acid. 3. Fill
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Acid Rain Lab Report Introduction: The problem was to see how crushed chalk and whole chalk weather differently. The independent variables are The temperature of the liquids The surface area of the chalk‚ crushed vs whole The dependant variable was the weathering of the chalk; this was calculated by measuring the foam reactant. Procedure: Part B- For the two partners recording data with the room temperature liquids‚ the materials where collected first. Two of the graduated
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