The Synthesis of Organic Aspirin ABSTRACT: The purpose of this experiment was to find out how a reaction undergoes for a globally known painkiller called aspirin‚ and to become familiar with achieving successful yields. Aspirin is synthesized from salicylic acid and acetic anhydride. Those two chemicals are mixed together along with sulfuric acid to form a crude solid. Filtration is used separate the impurities from the crude aspirin. To get purified aspirin‚ the precipitate was heated until all
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Organic Chemistry Laboratory Report. Experiment 1: Crystallization. Objectives: 1. To study the crystallization process. 2. To identify the best suitable solvent to use for the crystallization process. 3. Gain an experience in purifying an organic compound by the techniques of the crystallization. Introduction. Crystallization is a technique which chemists use to purify solid compounds. It is one of the fundamental procedures each chemist
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Unit 4 Assessment 2-Benzoic Acid Synthesis Synthesis and Investigation of Benzoic Acid Our aims: Create benzoic acid using benzaldehyde and hydrogen peroxide. Then remove some impurities from the benzoic acid crystals. Apparatus: Titration Pipette (25 cm3) Burette (50 cm3) Retort stand Clamp Conical flask (250 cm3) Volumetric flask (250 cm3) and stopper White tile Beakers (250 cm3) Dropping pipette Filter funnel Deionised water Phenolphthalein indicator Volumetric flask
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NORTHERN CARIBBEAN UNIVERSITY DEPARTMENT OF BIOLOGY‚ CHEMISTRY and ENVIRONMENTAL SCIENCE LABORATORY MANUAL Instructor: Dr. M. Wilson CHEM401: BIOCHEMISTRY for NURSES Prepared by: Oreane Collins CHEMISTRY LABORATORY REGULATIONS AND SAFETY PRECAUTIONS Reference: http://www.sciencebyjones.com/safety_rules.htm Thanks to the Flinn Scientific Safety Rules for much of the below. General Guidelines 1. Conduct yourself in a responsible manner at all times
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Being able to extract a compound or substance from a product or object will encourage us in being able to do the same in a similar manner with a tea solution. Extracting compounds is an important step in any kind of organic chemistry lab and will help us be better at accomplishing the experiment in a much faster and accurate rate than from before. Experimental To begin the experiment‚ a tea solution must be made by incorporating a tea bag into a beaker filled with almost boiling water and the
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10-fold dilution of this ionic iron solution and 5 drops of concentrated HNO3 was made. This solution served as the source of ionic Iron for the remainder of the lab and was labeled “stock ionic Iron solution.” Next‚ a 50-mL aqueous ionic Iron and FerroZine® complex solution was prepared by adding 5.00mL stock ionic Iron‚ 3-mL of acetic acid buffer‚ 2-mL of 5% hydroxylamine hydrochloride‚ allowing five minutes for hydroxylamine to reduce Fe3+ to Fe2+‚ adding 2.5-mL of 0.01 M FerroZine® solution‚ and
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Acetylsalicylic acid is the active pharmaceutical ingredient in aspirin and can be synthesized by the esterification reaction of salicylic acid and acetic anhydride in the presence of an acid catalyst. An esterification reaction is when an acid is converted into an ester by combining with an alcohol and removing a water molecule. When heating the salicylic acid mixture in the warm water bath‚ the mixture should be removed from the bath within 8 minutes‚ to reduce the chance of the acetylsalicylic acid decomposing
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Esterification Lab Introduction Esterification is an important part of organic chemistry that has many practical applications. Esterification can be used to make polymers. In most cases‚ esters are used for scents – they often smell fruity and sweet. In general‚ an esterification reaction results from a condensation reaction between a carboxylic acid and an alcohol. The carboxylic acid group loses an OH group‚ and the alcohol loses and H. For instance‚ the reaction between methanoic acid and methanol
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Caviness- Thames Lab Partner: Dena Jackson Reaction lab “I certify that this lab report is my own work‚ except for properly referenced and cited information. I have adhered to all guidelines published in the student handbook on Academic Integrity‚ as well as all guidelines published for this class in the Syllabus and Academic Integrity Handouts.” Purpose- The purpose of this lab was to display to us a variety of different reactions using an eclectic of things in the chemistry lab: including magnesium
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P. Stonebraker Organic Chemistry II lecture UCB Extension Spring 2013 Extra Credit Report Papers Paper is strictly optional. Write a 4-6 page paper on a subject approved by the instructor (either picked from the list below or picked by yourself). Emphasis in the paper should be on the organic chemistry associated with the subject (how it is synthesized‚ uses‚ etc.). No two students can research the same subject. Maximum value of the paper will likely in the 20-40 point range‚ depending
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