"Organic chemistry lab report perkin reaction alpha phenylcinnamic acid synthesis" Essays and Research Papers

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    Review  Packet  for  midterm  1                      10/2/2013   Nikki  Stefanko  &  Stephanie  Ventura     24   1.  Cortisol  is  a  steroid  hormone  produced  by  the  adrenal  cortex  that  is  released  in  response  to   stress  and  a  low  level  of  blood  glucocorticoids.     OH O OH HO H H

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    reacts with dilute acids. Planning What I am going to do I am going to find out how much heat is given out when magnesium reacts with a variety of dilute acids. In order to make comparisons between the acids‚ I shall use my results to work out how much heat would be given out if 1 mole of magnesium reacted with an excess of each acid. The acids I shall use are hydrochloric acid‚ sulphuric acid‚ nitric acid and ethanoic acid. What I already know Magnesium reacts with most dilute acids to give a magnesium

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    It is produced either as powdered or precipitated calcium carbonate. Calcium carbonate decomposes to calcium oxide and CO2 on heating. Treatment with dilute mineral acids produces corresponding calcium salts with liberation of CO2: CaCO3 + 2HNO3 Ca(NO3)2 + H2O + CO2(g) In this experiment‚ the mineral acid is added in excess to the calcium carbonate and the excess titrated against standard sodium hydroxide. This kind of titration is termed back titration. In this procedure

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    Prelab 5B Macrocyclic Synthesis OBJECTIVE: The objective this week is to produce Tetraphenylporphyrin and its metal complex. This will be carried out by condensation of 4 equivalents of Benzaldehyde and pyyrole in the presence of propanoic acid. The product will undergo UV/Visible Spectrum tests to determine its lambda max. The lambda max will show us the relationship between a conjugated system and the visible spectrum. PROCEDURE: Step 1: preparation of meso-tetraphenylporphyrin (TPP)

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    Kiley O’Toole Lab Report 3 Purpose The purpose of this lab was to uncover the number of layers of zinc atoms around a piece of galvanized iron. This was done by pouring the hydrochloric acid onto the galvanized iron‚ thus removing the zinc from the piece of metal. Laboratory Procedure 1. Measured and recorded the mass of a piece of galvanized iron using a centigram balance and a ruler 2. Measured and recorded the length and width of the galvanized iron using the ruler 3. Put the

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    prepare some simple organic compound and to purify the compound by recrystallisation. This experiment allowed the students to conduct the synthesis of aspirin‚ acquire the skills of recrystallisation using normal filtration and reinforce the technique of the melting point determination. The method used to synthesize aspirin was esterification by reacting salicylic acid with acetic anhydride with the presence of dehydrating agent‚ conc. sulphuric acid‚ to speed up the reaction. Having obtained the

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    The identification of acids and bases using a natural indicator Purpose: The purpose of this lab practice is to identify the pH of certain solutions and if they are acids or bases. Introduction: In chemistry‚ pH is a measure of the activity of the (solvated) hydrogen ion. p[H]‚ which measures the hydrogen ion concentration‚ is closely related to‚ and is often written as‚ pH. Depending on the pH solutions will be acids or bases. An acid is a chemical compound that dissociates in solution‚ releasing

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    Synthesis of Butyl Benzoate Using Phase Transfer Catalysis The objective of the experiment is to synthesize the butly benzoate by nucleophilic substitution and characterize it by IR spectroscopy. The percent yield of the final product is determined after the synthesis. Procedures: 2.0 mL of 1-bromobutane‚ 3.0 g of sodium benzoate‚ 5.0 mL of water‚ 4 drops of Aliquat 336‚ and a boiling stone were placed in a 50mL round-bottomed flask. The reaction mixture was refluxed for 1 hour and the flask

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    De-esterification for Synthesis of Benzoic Acid BATCH REACTOR Shane Bulk Chris Crosley David McGuire Max Skula Yunjing Song Shriram Sundarraj Nelson Zhou 155:416 Process Laboratory II Professor Jerry Sheinbeim January 28 – February 28‚ 2014 ABSTRACT The observed reaction that took place in this experiment was the de-esterification of ethyl benzoate to form benzoic acid. This experiment was used to determine the rate constant k of the synthesis of benzoic acid at different temperatures

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    Weak Acid Titration Abstract: Our method for determining the unknown weak acid was to determine the equilibrium constant K from the molecular weight of the weak acid from our titration data. In this lab the acid Potassium hydrogen phthalate and two unknown acids were titrated. We determined the molar mass of the Potassium hydrogen phthalate‚ for the unknown acids we calculated the molar mass and the Ka values. We used NaOH as the known base for titrating in all three of the titrations. Our

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