Locker# 1137 Date of Experiment: May 11‚ 2014 Date of Submission: May 16‚ 2014 Purpose: To determine the identity of an unknown hydrated salt calculating the percent water loss after heating and also to determine the empirical formula of magnesium oxide. Results: Table 1: Determination of the mass of waters of hydration of an unknown hydrated compound. Hydrated Compound code: C-14 Mass (g) Crucible + Lid 30.581g Crucible + Lid + Hydrated compound 31.590g Hydrated Compound 1.004g
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glittery |the sliver of magnesium. | | | | |(+) the liquid looks |(+) There was also a black |(+) The copper almost looks |(+) the balls of lead turned| |AgNO3 |ash-like and the Zinc turned|spot that appeared on the |like fuzz grew on it |black and look fuzzy and | | |black and looks like it is |magnesium. |
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The Grignard Synthesis of Triphenylmethanol Abstract: Grignard synthesis of triphenylmethanol was achieved by use of the Grignard reagent phenyl magesium brominde. The organometallic grignard reagent was synthesized by use of a reflux apparatus recrystallization techniques. Once synthesized it was used in a Grignard reaction that involved nucleophilic addition to a carbonyl in order to make triphenylmethanol. The final product was solidified and recrystallized and spectral data was
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The overall purpose of the lab is the understanding of the process and goals of the scientific method. This lab illustrates that this method is very useful to answer a question or address a problem base on observations and the available information. Hypothesis: There are more red marbles than black marbles. We were able to address our hypothesis with the data collected because 26.32% of the marbles are red and just 14.47% are black. Also‚ the percentage of red marbles is the biggest in comparison
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Purpose: To observe the reactions of specific aqueous solutions with specific aqueous reagents. Introduction: A solution is as a homogeneous mixture containing two or more substances. Reagents are added to solutions to create a chemical reaction or added to see if anything occurs. Reagents can be added to solutions to see if there is a presence of other substances. For example‚ iodine added to a lead solution. Iodine would be the reagent and would cause a chemical reaction confirming the presence
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The Grignard Synthesis of Triphenylmethanol Organic Chemistry Lab II March 19‚ 2012 Abstract The purpose of this experiment was to synthesize the Grignard reagent‚ phenyl magnesium bromide‚ and then use the manufactured Grignard reagent to synthesize the alcohol‚ triphenylmethanol‚ by reacting with benzophenone and protonation by H3O+. The triphenylmethanol was purified by recrystallization. The melting point‚ Infrared Spectroscopy‚ 13C NMR‚ and 1H NMR were used to characterize and confirm
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reaction‚ thus‚ of a chemical change. Materials Crucible tongs Evaporating dish Glass rod Test tubes Test tube rack Thermometer Analytical balance Magnesium ribbon pH paper 1M copper (II) sulfate Iron metal 6M hydrochloric acid Procedure Magnesium and oxygen test A small strip of magnesium metal is held on one end with a pair of crucible tongs‚ while the other end is ignited with the flame of Bunsen burner. The burning ribbon is held over a clean evaporating
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Writing Exercise – FePO4 Polymorphs 1. Compare and contrast the crystal structures and crystal chemistry of quartz‚ α-FePO4 and β-FePO4. FePO4 is a quartz-type of iron phosphate. It is different from other α-quartz isotypes due to the fact that the A-cation is a transition metal. The low-temperature α-phase can be from 294k neutron powder diffraction to high-temperature β-phase 1073K. As the quartz start to transit at 980K‚ from α-β‚ the Fe-O-P bridging angles start to increase value and the tetrahedral
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Factors Affecting Reaction Rate Lab Report Objective: To observe and record the different effects of reactants on concentration‚ surface area‚ and temperature‚ on the reaction rates for each. Materials: Refer to the Experiment 18A worksheet Procedure: Refer to the Experiment 18A worksheet Data Table: Mass of 11cm strip of Mg: 0.13g Average mass of 1 cm piece of Mg: 0.0118 Table 1: Effect of Concentration on Reaction Rate Concentration of Acid Reaction Time (s) Reaction
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Vu Ngo % MgO Determination September 10‚ 2012 Procedure: Reference to lab manual Data: Mass of Na2EDTA∙2H2O‚ g | .9289 | Standardization of EDTA Solution | Trial 1 | Trial 2 | Final buret reading‚ EDTA (mL) | 18.5 | 36.7 | Initial buret reading‚ EDTA(mL) | 0.5 | 18.5 | Determination of % MgO of Unknown Unknown Number | 4J | | Sample 1 | Sample 2 | Sample 3 | Mass of sample (g) | 0.2135 | 0.2132 | 0.2139 | Final buret reading‚ EDTA (mL) | 73.5 | 74.2 | 74.2 | Initial
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