Distillation Purpose: To conduct the distillation process‚ simple or fractional. Procedure: 1. Add 5ml of 20% ethanol: water mix to the distillation flask. 2. Add 23 stir bar 3. Make sure that the thermometer bulb is just below the Claisen Head‚ carefully. Be very gentle with the thermometers and take care not to break them. 4. Label 3 vials‚ 1‚2‚ and 3. 5. Place receiving vial 1 on ice to collect the distillate 6. Start the distillation by piling up hot sand around the distillation flask with
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Name of the Experiment: Simple Distillation (Semimicroscale Procedure.) Abstract: Distillation is a method of process of separating 1:1 mixture based on differences in their volatilities in a boiling liquid mixture. Distillation is done with the use of simple distillation apparatus shown in Figure 1. In this experiment‚ simple distillation process was used to determine the identities of the unknown compounds in the solution through the obtained boiling points. The list of probable unknown volatile
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Simple Distillation Experimental Organic Chemistry: A Miniscale and Microscale Approach. 4th Edition. By Gilbert and Martin. Section: 4.4 Introduction: Distillation is a technique used to purify various liquids. In a simple distillation‚ a liquid is boiled and the vapors work through the apparatus until they reach the condenser where they are cooled and reliquified. Liquids are separated based upon their differences in boiling point in which each pure substance is at least greater than 40-50
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therefore then allowing toluene particles to separate in the later fractions when temperature is over 105 degrees Celsius. Lastly‚ it is concluded that fractional distillation is a more effective method as opposed to simple distillation because in fraction 7 of the simple‚ there was only around 36% toluene consumption versus a 96% in the fractional distillation. This is also due to the fact that using a fractionating column makes the samples more pure because it works better at separating the first couple
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eugenol in the basic aqueous layer‚ and acetyleugenol in the organic layer. The basic aqueous layer can be acidified to re-extract eugenol from it. And the organic layer can be dried and concentrated to yield acetyleugenol The principle of steam distillation is based on the fact that two immiscible liquids will boil at a lower temperature than the boiling points of either pure component‚ because the total vapor pressure of the heterogeneous mixture is simply the sum of the vapor pressures of the individual
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In the experiment of distillation we separated two miscible liquids. The purpose of distillation is to identify and purify compounds. We began our experiment by setting up an apparatus for macroscale simple distillation. We used 60 ml of Cyclohexane/ Toluene. We began with the temperature at 50 degrees Celsius. Unfortunately‚ we reached an error when the compounds evaporated too rapidly. The compounds evaporated so quickly that we lost data from 2 ml to 13 ml. The heat was lowered and as a result
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Distillation Column In the the Chemical Enginneering Lab at CSULB there is a total reflux eight-stage glass binary distillation column at atmospheric pressure. The components that need to be separated are 1-propanol and 2-propanol. These two compounds are isomers with fairly close boiling points. They are separated based on their physical propertis. With the
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FRACTIONAL RESERVE BANKING Fractional reserve banking is a system under which bankers keep as reserves only a fraction of the funds they hold on deposit. This system has three features: • Bank Profitability By getting deposits at zero interest and lending some of them out at positive interest rates‚ goldsmiths made profits. The history of banking as a profitmaking industry was begun and has continued to this date. Banks‚ like other enterprises‚ are in business to earn profits. • Bank Discretion
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Steam Distillation Purpose: To use steam distillation to purify heat sensitive‚ natural products‚ like essential oils. Procedure Please refer to: Williamson‚ Macroscale &Microscale Organic Experiments 4th Ed.‚ pgs.98-109 Results Table 1.1: Steam distillation Drop # (every third drop) Temperature (ºC) Addition of 0.5 mL water 1 100.3 Water added 2 100.5 3 100.5 Water added 4 100.6 Water added 5 100.6 6 100.6 Water added 7 100.6 8 100.6 Water added 9 100.3 10 100.6
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All about Distillation Distillation is a process that is used to purify a lot of substances on a domestic as well as commercial basis. It is very interesting to know about the process in detail as it is a natural process. The story begins when a liquid or solid state of mater responds to the heat in environment. The heat makes the liquid state or solid state of matter to convert into gas state. Liquid Gas (Vaporization) Solids
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