CHAPTER I INTRODUCTION 1.1 HISTORY: Ethylene Glycol (1‚ 2 – ethanediol)‚ HOCH2CH2OH usually called glycol is the simplest Diol. Diethylene glycol and Triethylene glycol are Oligomers of Mono ethylene glycol. Ethylene glycol was first prepared by Wurtz in 1859; treatment of 1‚2 dibromoethane with silver acetate yielding ethylene glycol diacetate via saponification with potassium hydroxide and in
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Jacobsen’s Method of Epoxidation of an Alkene | | Abstract Various types of reactions were completed to first create and then use Jacobsen’s catalyst in the asymmetric epoxidation of an unknown alkene with bleach in the laboratory. The chiral epoxide synthesized was then characterized with GC/MS and NMR. With this information the unknown alkene was able to be identified as 4-chlorostyrene. Introduction Organisms have evolved with mechanisms that use specific enantiomers of molecules
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Background of the Study Tea is created by using the leaves of a plant known as Camellis sinensis. This plant is native to mainland China‚ South and Southeast Asia‚ but it is today cultivated across the world in tropical and subtropical regions. It is an evergreen shrub or small tree that is usually trimmed to below 2 m (6.6 ft) when cultivated for its leaves. It has a strong taproot. The flowers are yellow-white‚ 2.5-4cm (0.98-1.6 in) in diameter‚ with 7 to 8 petals. Tea-drinking can be traced back
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PbCO3(soluble in 6M HCl‚ soluble in sln of good complexing agent) | Blue ppt‚ CuCO3(soluble in 6M HCl‚ soluble in sln of good complexing agent) | Green ppt‚ NiCO3(soluble in 6M HCl‚ soluble in sln of good complexing agent) | White ppt‚ BaCO3(soluble in 6M acetic acid‚ soluble in 12M HCl) | NH3 | Brown ppt‚ Ag2O(soluble
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methosulfate (186 μM)‚ 0.3 ml of nitro blue tetrazolium (300 μM) and 0.2 ml of NADH (750 μM) were mixed together. The reaction started by addition of 0.2 ml of NADH. After incubation at 30 ̊C for90s‚ the reaction stopped by the addition of 0.1ml of glacial acetic acid. 2.10. Catalase activity assay Abei’s method [27]was used for Measurement of Catalase activity. 5μl of tissue lysis was
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Experimental Part 1: Reaction First the glassware apparatus for the reaction was set up. 3.861-grams of isoborneol‚ 2.21-mL of glacial acetic acid‚ and 4.39-mL of 6% NaOCl solution were mixed in a 125-mL Erlenmeyer flask. Another 35-mL of 6% NaOCl solution was added to a separatory funnel and supported over the flask. The NaOCl in the sep funnel was slowly added into the Erlenmeyer flask with vigorous swirling‚ approximately 2-mL every 30 seconds until all the NaOCl from the sep funnel had been
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Chemistry 3373F Lab Manual 2008 Modified 11/07 Table of Contents Chem 3373 Laboratory Schedule for Fall 2008.............................................................................2 The Benzoin Condensation of Benzaldehyde ..............................................................................3 Synthesis of Dilantin and Related Compounds (two weeks).........................................................6 Synthesis of an Alkaloid: Pseudopelletierine (two weeks) .............
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Ronak Parikh U30682934 Experiment 2: Diels-Alder Reaction: Synthesis of cis-Norbornene-5‚6-endo-dicaroboxylic anhydride Introduction: The main goal of this experiment is to perform a Diels-Alder reaction between 2‚3-dimethyl-1‚3-butadiene and maleic anhydride‚ identify the product and hydrolyze to form the dicarboxylic acid. Diels alder reactions are classified as pericyclic reaction‚ which is a reaction which involves a cyclic rearrangement of bonding electrons‚ which means
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TETRAHEDRON LETTERS Tetrahedron Letters 39 (1998) 9279-9282 Pergamon Efficiencies of Reductive Amination Reactions on Different Solid Supports Chinh T Bui‚ Firas A. Rasoul‚ Francesca Ercole‚ Yen Pham and N Joe Maeji* Cluron TechnologiesPry Ltd.. 11 Duerdin Street. Cla.~aon‚Vic. 3168‚ Australia Received 12 August 1998; accepted 1 October 1998 Abstract: Rreductive amination on resins derivatized with 5-(4-forntyl-3‚5-dimethoxyphenoxv)valeric acid linker (Barallv linker‚ 1) 1 has been
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