Experiment 1: Recrystallization – Evaluation Summary Last Name: Xavier First Name: Jessica Date: October 1st 2013 Lab Day/TA/Group: Wednesday(1:35pm)/Group A Labs reports must be typed and chemical structures must be drawn with ChemDraw. Report must not exceed three pages (including this page). Page limit does not include any attached spectra or references. ** Deductions for hand written report/structures and exceeding page limit ** Report Breakdown Data/Results: _________________
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The objective of this experiment was to learn the process of recrystallization and how this process removes the impurities from a pure solid compound. The methods used to achieve this objective were also hot vacuum filtration in order to remove suspended solid impurities‚ and isolating the pure acetanilide. In the next lab‚ percent recovered was obtained through weighing the acetanilide sample as well as comparing its melting point range. In this experiment‚ the sample‚ acetanilide was weighted
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Exercise No. 8 CARBOXYLIC ACIDS AND ACID DERIVATIVES I. OBJECTIVES: • To investigate the physical and chemical properties of Carboxylic acid and its derivatives • To understand the reactions of carboxylic compounds and derivatives. II. EXPERIMENTAL RESULTS Solubility of Carboxylic acids in 10% NaHCO¬3 Acetic acid - formation of bubbles Benzoic acid - formation of bubbles Test for Acetic acid NaOH + Acetic acid - blue litmus paper turned red NaOH + Acetic acid + FeCl3 - red colored
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by everyday pollution from houses‚ factories‚ cars‚ and etc. This is the concept of acid rain‚ which according to EPA.gov is a broad term referring to a mixture of wet and dry deposition from the atmosphere containing higher than normal amounts of nitric and sulfuric acids. Acid rain isn’t just rain‚ its forms like hail or snow‚ which is wet deposition‚ and smoke or dust‚ which is dry deposition. The effects of acid rain are quite terrifying bringing all types of problems to the Earth‚ for example
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Acid Base Titration bre’ana March 1‚ 2013 Purpose: The purpose of this experiment is to determine the concentration of a solution of NaOH by titration with a standard solution of HCl. It was also the purpose to determine the concentration of a sample of white vinegar by titration with a standard solution of NaOH. Introduction: Using the method of titration is how the experiment gets to the conclusion of the concentration of a solution. When doing this experiment‚ measurement is very important
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Chem 231: Organic Chemistry Lab EXPERIMENT #2 and #3 Extraction and Evaporation Recrystallization and Melting Point Measurement PURPOSE: 1. To the components of a simulated pharmaceutical preparation‚ Panacetin‚ and identifying the unknown component of the mixture through extraction and separation methods. 2. To learn how to purify by recrystallization‚ how to dry them and how to obtain a melting point. PRECAUTION: ACETANILIDE AND PHENACETIN ARE EYE AND SKIN IRRITANTS. Minimize
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Synthesis of Salicylic Acid Experimental Data: 1. Mass of methyl salicylate used: 0.232 g 2. Theoretical yield of salicylic acid: 0.211 g 3. Volume H2SO4 added‚ with units (drops or mL): 3mL 4. Mass of crude salicylic acid obtained: 0.250 g 5. Volume of water used as recrystallizing solvent: 2 mL 6. Mass of purified salicylic acid: 0.134 g 7. Percent yield of purified salicylic acid from reaction: 63.5% 8. Melting point of purified product: 158-160 oC 9. Name of NMR solvent used and
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The Purity and Purification of Solids Recrystallization ABSTRACT In this experiment‚ impure adipic acid is purified though recrystallization. The impure adipic acid is dissolved in a solvent. After cooling it is ran through a vacuum filter to separate any moisture. The dry crystals are then weight for percent yield and the melting point range is taken to test the purity. There were two different trials ran in this experiment. The difference between the two was the addition of charcoal in
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A carboxylic acid is an organic acid characterized by the presence of at least one carboxyl group. The general formula of a carboxylic acid is R-COOH‚ where R is some monovalent functional group. A carboxyl group (or carboxy) is a functional group consisting of a carbonyl (RR’C=O) and a hydroxyl (R-O-H)‚ which has the formula -C(=O)OH‚ usually written as -COOH or -CO2H. Carboxylic acids are Brønsted-Lowry acids because they are proton (H+) donors. They are the most common type of organic acid. Among
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Recrystallization is the process in which a chemical compound becomes a solid. The difference between recrystallization and the presence of precipitate is the structure. In Cystristalizatqion the solid compound contain a crystal-like structure. According to Hill and Barbaro the most common method of purifying organic compounds. Not only does recrystallization allow people with the ability to converting organic molecules to crystal-like solids. This process is performed in the creation of rock candy
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