CHM 2046 L Scheme of Analysis for Unknown 9A/9B “Fair Game” Unknowns * Cations: Na+‚ K+‚ NH4+‚ Ca2+‚ Mg(H2O)62+‚ Al(H2O)63+‚ Zn(H2O)62+‚ Cu(H2O)2+‚ Ag(H2O)+ * Anions: Cl-‚ NO3-‚ SO4-2‚ HSO4-‚ OH-‚ CO3-2‚ HCO3-‚ S-2 * Insoluble Salts: Ca(OH)2‚ CaCO3‚ CaSO4‚ Mg(OH)2‚ MgCO3‚ Ag2O‚ AgCl‚ Ag2S‚ CuO‚ CuCO3‚ CuS‚ Zn(OH)2‚ ZnCO3‚ ZnS * Alums: [Al(OH2)6]2(SO4)3∙6H2O‚ Na[Al(OH2)6](SO4)2∙6H2O‚ K[Al(OH2)6](SO4)2∙6H2O‚ NH4[Al(OH2)6]2(SO4)2∙6H2O * Hydrated Ions: Na2CO3∙10H2O‚ Na2SO4∙10H2O
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put into the flask. Water was then added to the same flask. Then phenolphthalein indicator solution was added before we began titrating by adding more drops of the NaOH solution while swirling the flask until a pink color remained. The liquid levels were recorded on both burets. Part B: Solid unknown acid was added to a flask with water and swirled until almost fully dissolved. Then phenolphthalein indicator was added. With standardized NaOH solution we titrated and recorded the initial and
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to the mark with distilled water and then ensure that the contents of the flask are well mixed by repeated shakings. c. Titrate 25 cm3 portions of the diluted reaction mixture with the standard 0.050 M sulphuric acid provided‚ using phenol red indicator until two or three consistent results are obtained. d. Calculate the weight of acetylsalicylic acid in each tablet and compare your results with the manufacturer’s specification. Compare your results with those given in different brands of aspirin
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Oxidation Reduction Titrations: The Indirect Iodimetric Analysis Ascorbic Acid Unknown Number 69 I: Purpose: To determine the percent weight of Ascorbic Acid in unknown sample. This was to be done by the means of an indirect iodimetric analysis. In an iodometric analysis‚ the oxidizing agent can be determined by a different means than titrating directly with standard iodide‚ because a high concentration of I- is needed to form the I3- complex. In this type of analysis‚ excess iodide is added to
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~1/2-2/3 of sample in ~10-15mL of DIW. Always retain a sample of original sample! This sample/DIW ratio will give ion concentrations of ~0.1-0.2M for soluble salts of unknowns. (ii) Observe pH to one SF Use small portion of sample to make a solution with neutral water to test pH with indicators. ≈2 HSO4- (no OH-) ≈5-6 NH4+ ≈7 Cl-‚ NO3-‚ SO42-‚ Na+‚ K+ ≥13 OH- (iii) Perform necessary separations If Na+ and NH4+ are present‚ testing for K+ requires separation of NH4+. Place
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is also widely known as neutralization. In this experiment‚ we used titration technique which involves accurately measuring the volume of a solution required to react with another reagent. An indicator must be used to determine the end point of the titration. The indicator used can change colors at different pH values. OBJECTIVE To determine the concentration of sulphuric acid (H2SO4) using titration technique CHEMICALS NaOH solution‚ approximately 0.2 M‚ dilute sulphuric acid of unknown molarity
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Investigating the effects of acid rain in the growth of cress seedlings IntroductionAcid rain is rain or any other form of precipitation‚ which is unusually acidic. It has harmful effects on plants‚ animals and buildings. Acid rain is mostly caused by human emissions of sulphur and nitrogen compounds which react in the atmosphere to produce acids. Acid rain can slow the growth of vulnerable forests and cause leaves and needles to turn brown and fall off. In addition‚ it depletes minerals from the
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Cyra Vose Klebsiella Pneumoniae #34 MCB 2010C Friday 9:00am Introduction: On November 16‚ 2012 at 0900 I was given case #34. Mr. Joe Blough presented with a sudden high fever (103 degrees Fahrenheit or higher) and mentioned he felt dizzy and had the chills. During this visit Mr. Blough seemed to be coughing and producing sputum. This sputum was thick and had some blood present. I had my assistant collect a sample of the sputum so we could run some tests and hopefully correctly diagnose Mr. Blough
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solvents. Statement of purpose We would like to know whether permanent marker ink is removable by any of the solvents we are going to use in our experiment‚ which are ethanol‚ water‚ acetic acid‚ and soap water. We would also like to know whether the pH scale of a solvent or whether they are polar or non-polar substances can affect the result of
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Lewis acid‚ thus playing a role as a ligand. The indicators used in EDTA titrations are metal ion indicators. Metal ion indicators work by the presence of absence of metal ions. Just like EDTA‚ the metal ion indicators will bind with metals. When the titrations begin‚ Mg2+ will be formed in a complex with the indicator. Once EDTA is added‚ it binds to the free Mg2+ ions‚ and then it reacts with the Mg2+ ions that are already bound to the indicator. When the EDTA is added‚ the solution will turn red
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