Top-Rated Free Essay
Preview

Several methods of dewaxing and the operation process is introduced

Satisfactory Essays
305 Words
Grammar
Grammar
Plagiarism
Plagiarism
Writing
Writing
Score
Score
Several methods of dewaxing and the operation process is introduced
Meathod dewaxing process:
Meathod is the use of wax molecules at low temperature of hydrophilic, enrichment of wax molecules by dilute alkali liquor, and wax crystallization.Oil, acid less than 0.05% (FFA) in 15 ℃ or so into the crystallizer, refrigerant cold quickly to 1 ~ 7 ℃ and with low shear force and high cycle blender mixing, promote wax crystallization.Again according to the rice bran extract (http://www.ricebranoilplant.com) concentration of 20% ~ 40% to 1% ~ 3% of the low temperature lye, to keep temperature not to exceed 8 ℃, agitating continuously 15 ~ 20 minutes, drive centrifuge separation after demulsification.Its operation is the key, phosphoric acid and adding method at low temperature.
Method of coagulant dewaxing process:
By the method of coagulant dewaxing, frozen waxy oil is to 9 ~ 13 ℃, then stir, add theory alkaline neutralization of free fatty acids.Concentration of 15 ° alkali used Be 'left and right sides, stir in 60 ~ 70 RPM cases 1 ~ 1.2 hour, add 0.1% of the oil heavy aluminium sulfate (aqueous solution with the concentration of 13.6% ~ 13.6%), continue to stir 1 ~ 1.2 hours, terminal temperature shall not exceed 17 ℃, and then after the separation, XianDi and drying, for a quick dewaxing oil products.
The operation of the urea dewaxing process:
Urea dewaxing method is by adding urea solution containing wax molecules cocrystallization a dewaxing method.Will first waxy oil alkali refining by conventional method, and then cold from around 10 ℃, dispersant 3% of urea (with a saturated aqueous solution), stir crystallization 20 ~ 24 hours, the centrifugal separation, washing and drying for a quick dewaxing oil products.
Urea dewaxing method and conventional method namely pure kernel recycle station (http://www.palmmill.com/Products/prod/) equipment general, dewaxing rate is higher, the residual urea removal can be combined with subsequent working procedure, but the urea decomposition product ammonia caused environmental pollution, remains to be further perfect technology and equipment.

You May Also Find These Documents Helpful

  • Powerful Essays

    Dissolve the solid in exactly 4 mL tert-butyl methyl ether of. Add exactly 2 mL of water, cap the tube and shake. Let the mixture stand until two layers are formed. Remove the aqueous layer. Wash the organic layer two more times with exactly 2 mL of water (each time). After the final wash, dry the organic layer with calcium chloride pellets. Remove the ether with a pipette and filter through a funnel plugged with cotton into a pre-weighed 50 mL beaker including a boiling chip. Wash the pellets with a full pipette of ether. Remove the ether with a pipette and filter through the funnel plugged with cotton into the 50 mL beaker. Evaporate off the ether in the hood on a hot plate under low heat. When the beaker has cooled to room temperature, weigh the…

    • 2981 Words
    • 12 Pages
    Powerful Essays
  • Good Essays

    100 ml water mixed with 10 ml vegetable oil filtered through cheesecloth and 60 ml of soil oil appeared to be filtered out by process and 70 ml was captured in beaker…

    • 1060 Words
    • 5 Pages
    Good Essays
  • Good Essays

    The heavy crude oil extracted from oil sands is a viscous semisolid that does not easily flow at normal oil pipeline temperatures, making it difficult to transport to market and expensive to process into gasoline, diesel and fuel. It must be either mixed with lighter petroleum or chemically split…

    • 784 Words
    • 4 Pages
    Good Essays
  • Better Essays

    Diels Alder Reaction Lab

    • 1246 Words
    • 5 Pages

    Use aluminum foil to insulate between the flask and the bottom of the reflux condenser and be sure to attach a drying tube with anhydrous calcium chloride. Heat the solution between 150 – 155oC, once at this temperature; keep it there for 20 minutes and avoid overheating. Then allow the mixture to cool to room temperature. Transfer contents to a 25mL Erlenmeyer flask and add 3mL of toluene (if the crystals do not dissolve then the contents may be heated). Add about 3mL of petroleum ether until slight cloudiness continues then heat the flask until the solution is clear. Crystals should form as the solution cools to room temperature, then you may put on an ice bath to complete crystallization. (Using vacuum filtration) Wash the product with approx. 5mL of cold petroleum ether and allow the product to completely dry over the next week (so an accurate weight and melting point may be…

    • 1246 Words
    • 5 Pages
    Better Essays
  • Better Essays

    alcohol (2-methyl-2-butanol, MW _ 88.2, d _ 0.805 g/mL) and 25 mL of concentrated hydrochloric acid (d _ 1.18 g/mL). Do not stopper the funnel. Gently swirl the mixture in the separatory funnel for about 1 minute. After this period of swirling, stopper the separatory funnel and carefully invert it. Without shaking the separatory funnel, immediately open…

    • 952 Words
    • 4 Pages
    Better Essays
  • Good Essays

    Weigh 150 mmol of isopentyl alcohol into a round bottom flask of appropriate size, and add boiling chips. Under a hood, add 17 mL of glacial acetic acid, and then carefully mix in 1.0…

    • 1073 Words
    • 5 Pages
    Good Essays
  • Good Essays

    Dissolve 25.0 mmol of vanillin in 30 mL 1 M sodium hydroxide in a 125 mL Erlenmeyer flask. If the mixture does not dissolve after 5 minutes of continuous stirring, add another 5 mL sodium hydroxide. Cool the solution to just below 15 oC. In a small beaker, dissolve 12.0 mmol of sodium borohydride in about 6 mL of 1 M sodium hydroxide. Remove the vanillin solution from the ice bath, and add the sodium borohydride solution in small portions to the vanillin over a 5 minute period. Make sure the temperature of the vanillin solution stays in the range of 20-25 oC. (In fact, this is the ideal temperature range for the rest of the lab, through acidification and initial crystal formation.) Once all of the sodium borohydride has been added, let the solution sit at room temperature for 30 minutes, with frequent swirling. Acidify the solution with 6 M hydrochloric acid (6-10 mL may be required), keeping the temperature between 20 and 25 oC. Perform this step carefully, as the solution will foam and the foam will contain vanillyl alcohol. Also, if the mixture gets too hot at this stage, the product will not crystallize properly. Check the pH with litmus paper to ensure it is acidic. Once crystal formation has begun, cool the mixture in the ice bath for 15 minutes. Collect the vanillyl alcohol by vacuum filtration, and wash the crystals with cold water. Store the product in a container specified by the instructor…

    • 491 Words
    • 2 Pages
    Good Essays
  • Good Essays

    The liquid was mixed by vortexing the tube few times and centrifuged for 2 minutes. The supernatant was discarded. Next, 600 μl of 70% ethanol at room temperature was added and mixed gently. The tube was centrifuged for 2 minutes at max speed. Next, the ethanol was removed and the pellet was dried for 10-15 minutes.…

    • 918 Words
    • 4 Pages
    Good Essays
  • Good Essays

    Result and CalculationMass of aldehyde #1 (starting material) = 0.3999 gMass of alcohol #1 (product) = 0.1573 g alcoholTheoretical yield = 0.3999 g vanillin x (154.17 g alcohol/152.15 g vanillin) = 0.4052gPercentage yield = (actual yield/theoretical yield) x 100%= 0.1573 g alcohol/ 0.4052 g alcohol = 38.8%Solvent system chosen = ethyl acetate and hexane in 9:1 ratioMelting point range of alcohol #1 = 108oC -109oCObservationWhen the NaOH was added to the aldehyde #1, the solution turned yellowish green. It took 10 minutes for the white solid NaBH4 to completely dissolve in the aldehyde solution. When the HCl was added, the solution fizzed and bubbles came off. White precipitate formed. After the vacuum filtration, shiny white crystalline solid was found.…

    • 547 Words
    • 2 Pages
    Good Essays
  • Good Essays

    After complete addition of the sodium hydroxide, the mixture was left to stir for a further 30 minutes after which we reduced the stirrer speed to a gentle spin and water (2ml) was added and then stirred for a few more minutes. The content was transferred to a separatory funnel (30ml), using water (5ml) and dichloromethane (5ml) to complete the transfer. The mixture was shaken and left to settle, the organic layer was removed to an Erlenmeyer flask and the aqueous layer was extracted once more with dichloromethane (5ml) and then combined with the previous organic extract. The combined organic layers were dried with anhydrous sodium sulfate, transferred through a Hirsch funnel into a filter flask (25m) attached to an aspirator. Filter paper was used to stop the drying agent from passing through the funnel, and the Erlenmeyer was rinsed with dichloromethane (1ml) and was poured over the drying agent in Hirsch funnel. After all the solvent went in the filter flask the aspirator was turned off, and the filter paper with…

    • 697 Words
    • 3 Pages
    Good Essays
  • Good Essays

    An oil maceration is the product of plant matter being soaked in a carrier oil. A carrier oil is an unsaturated fat that is liquid at room temperature such as olive, and avocado oil. The preferred carrier is fractionated coconut oil because it has been distilled which makes it sterile and have a shelf-life of up to six years. This procedure starts…

    • 338 Words
    • 2 Pages
    Good Essays
  • Satisfactory Essays

    Making a Paracetamol

    • 307 Words
    • 2 Pages

    * After drying, the crude product should be placed in a clean 100cm3 conical flask and recrystalised by heating until it just dissolves in approximately 20cm3 of water.…

    • 307 Words
    • 2 Pages
    Satisfactory Essays
  • Good Essays

    Effects of Oil Spills

    • 339 Words
    • 2 Pages

    There are 3 main ways to separate oil from water and 3 absorbents that can be used. The first way to remove oil is A belt, hose or disc, moves through a layer of oil, which causes the oil to adhere to the surface and be carried off. The second way is to Coalesce which is when smaller oil drops in an oil/water mixture will separate slowly or not at all. Coalescing media is placed in an oil separator to catch and accumulate the finer oil drops then merge them into larger drops that separate quickly. The third way is where the three absorbents come in which is Gravity separation, which is a fancy way of saying the oil and water layers are prominent. Two of three of the absorbents are fairly fast at removing oil. The third, well helps decompose the oil faster. The first absorbent is human hair, most people can see why because it grasp onto oil and keeps it but that way is kind of messy. The second absorbent is Saw dust which is a little cleaner then the hair but just about as messy. The third way which dose not really absorb as much as decompose the oil is using pure nitrogen and phosphorus to form little Tar balls which aren’t as deadly to the environment as the liquid crude oil. But no there is a forth absorbent let to be endorsed by the government. It is a polymer called WENV-250 and it was developed by a scientist to remove oil more defiantly. The polymer is non toxic so it may be used to put on birds feathers then simply pulled…

    • 339 Words
    • 2 Pages
    Good Essays
  • Good Essays

    Manganese Lab Report

    • 1363 Words
    • 6 Pages

    Place a small glass funnel in the mouth of the flask to serve as a reflux condenser, and boil on a steam bath for 5 minutes. Carefully decant the solution into a 100 mL Erlenmeyer, leaving any solid residue behind, and add 5 mL of methanol. Reheat to dissolve, then cool to room temperature. Isolate the product by suction filtration. Wash with a little ice-cold methanol, and suction dry, then air dry.…

    • 1363 Words
    • 6 Pages
    Good Essays
  • Satisfactory Essays

    Prepare the ingredients and materials needed. Scrape the gel of the aloe vera and put ut in a bowl. After scraping the gel, put it in a plastic container and add 1 cup of ethyl alcohol and 2 tsps. of glycerin. Next, use the mortar and pessel to smash the malunggay leaves. After smashing the malunggay leaves, squeeze it to get its extract. Then, add the malunggay extract to the plastic container and mix it till well blended. Then, smash the sampaguita flowers and squeeze it to get its extract and add it into the mixture. Lastly, put the product in an empty hand sanitizing bottle. Apply a little amount of the product to your hand to remove bacterias and makes your hand fragrant.…

    • 731 Words
    • 6 Pages
    Satisfactory Essays

Related Topics