Preview

Observing Reactions of Sulfuric Acid

Good Essays
Open Document
Open Document
579 Words
Grammar
Grammar
Plagiarism
Plagiarism
Writing
Writing
Score
Score
Observing Reactions of Sulfuric Acid
Assessment task 3 oral presentation summary
Description of the experiment * Aim: To observe the reactions of sulfuric acid as an oxidising agent and as a dehydrating agent.
Equipment:
* 20mL of concentrated sulfuric acid * 20mL of 2mol/L sulfuric acid * 2 small pieces of each of copper, zinc and iron * Sandpaper * 10 test tubes * Test tube rack * 2g of sugar crystals (sucrose) * 2 wooden ice-cream sticks * 10mL measuring cylinders
Steps:
A: Sulfuric acid as an oxidising agent 1. Clean pieces of metal with sandpaper to remove oxide coating. 2. Add a piece of each metal to a separate test tube. 3. Add 5mL of concentrated sulfuric acid to each test tube. 4. Record the observations. 5. Repeat the experiment with 2mol/L sulfuric acid.
B: Sulfuric acid as dehydrating agent 1. Place 1g of sugar (sucrose) and a wooden ice-cream stick into separate test tube. 2. Add 1-2mL of concentrated sulfuric acid to each test tube. 3. Record the observations. 4. Repeat the experiment with 2mol/L sulfuric acid

Risk assessment * Conc. sulfuric acid is highly corrosive * If conc. Sulfuric acid is spilt, do not add water * Hydrogen sulfide gas

Results | Observations | | Conc. Sulfuric acid | 2 mol/L sulfuric acid | Copper | No observable change | No observable change | Zinc | No observable change | No observable change | Iron | * Exothermic reaction * Bubbling gas | No observable change | Sugar | * Exothermic reaction * Black solid is produced and pushed out from the test tube * Gas with rotten egg smell is released | No observable change | Wood | * Black layer is formed on the wood | No observable change |
Validity and reliability * Experiment was not repeated * Low reliability * Results not consistent with the known theory * Invalid * Require to eliminate experimental errors

Analysis of the results
HSC syllabus



Bibliography: 1. 2012books.lardbucket.org (n.d.) Untitled. [image online] Available at: http://2012books.lardbucket.org/books/general-chemistry-principles-patterns-and-applications-v1.0/section_18/65faa2f875a51b122536441d9c6a90d2.jpg [Accessed: 14 May 2013]. 2. angryewan (2008) Sulfuric acid in sugar. [video online] Available at: http://www.youtube.com/watch?v=_gG0UAX3V7c [Accessed: 14 May 2013]. 3. cellbiologyolm.stevegallik.org (n.d.) Untitled. [image online] Available at: http://cellbiologyolm.stevegallik.org/sites/all/images/sucrose.png [Accessed: 14 May 2013]. 4. Tregarthen, L. (2003) HSC Chemistry. 3rd ed. South Yarra: Macmillan Education Australia Pty Ltd, p.P.118-119. 5. www.docbrown.info (n.d.) Untitled. [image online] Available at: http://www.docbrown.info/page04/OilProducts/esterprep1.gif [Accessed: 14 May 2013]. 6. www.weneedsigns.com (n.d.) Untitled. [image online] Available at: http://www.weneedsigns.com/images/C/Danger%20Sulfuric%20acid.jpg [Accessed: 14 May 2013].

You May Also Find These Documents Helpful

  • Good Essays

    Experiment 13B

    • 972 Words
    • 4 Pages

    A reflux condenser was assembled using a 25-mL round-bottom flask, hot plate, and aluminum block. It was equipped with a drying tube filled with calcium chloride to control vapors. Approximately 2.5 mL of isopentyl alcohol was massed and placed in the round-bottom flask that contained a stir bar. Using the same graduated cylinder, about 3.5 mL of glacial acetic acid was added to the flask. A calibrated Pasteur pipet was used to add 0.5 mL of concentrated sulfuric acid to the flask and the flask was mixed immediately. The flask was connected to the apparatus and covered with aluminum foil to help retain heat. Using rubber tubing, water was circulated into the lower attachment and out the top attachment and the mixture was brought to a boil. After heating under reflux for 60-75 minutes, the flask was removed from the heating source and left to cool down to room temperature. The reaction mixture from the flask was transferred to a culture tube and 5-mL of water was added. Upon addition of water, careful shaking, and occasional venting, the phases separated and the lower aqueous layer was removed and discarded. Using the same procedure as explained above with water, 2.5 mL of aqueous sodium bicarbonate was added and the lower aqueous layer was again removed and discarded. The same procedure was repeated one last time with 2.5 mL of saturated aqueous sodium chloride and the lower aqueous layer was removed and discarded, leaving behind the crude ester. The crude ester was transferred to…

    • 972 Words
    • 4 Pages
    Good Essays
  • Better Essays

    EDMG 240 Paper

    • 1019 Words
    • 3 Pages

    Editors of Encyclopedia Britannica. (2014, January 12). sulfuric acid (chemical compound). Encyclopedia Britannica Online. Retrieved July 24, 2014, from http://www.britannica.com/EBchecked/topic/572815/sulfuric-aci…

    • 1019 Words
    • 3 Pages
    Better Essays
  • Good Essays

    Lab: Synthesis Of Esters

    • 573 Words
    • 3 Pages

    Procedure- Prepare a hot-water by half filling a 500-mL beaker with water and heating it carefully on a hot plate until it comes to a gentle boil. Number the test in the rack in order you will put the Alcohols in them. Then create a table and write down all the Alcohols in the order you receive and use the table to record your observations. Now place 1mL of specific Alcohol in each of the test tubes. After putting the Alcohols put 1mL of Acetic Acid in each of the test tube. Now finally add 0.5mL of concentrated Sulphuric Acid to each of the test tubes. Now gently shake…

    • 573 Words
    • 3 Pages
    Good Essays
  • Powerful Essays

    Ely Mine

    • 1764 Words
    • 14 Pages

    Seager, S. L., & Slabaugh, M. R. (2000). Chemistry for Today (4th Ed.). Pacific Grove, CA: Brooks/Cole.…

    • 1764 Words
    • 14 Pages
    Powerful Essays
  • Powerful Essays

    In a 50 mL round bottom flask, 7.5mL of Isoamyl Alcohol, 4.0 mL of 17.4M Glacial Acetic Acid, 1 mL of concentrated Sulfuric Acid, and 6.9 mL of Hexane were combined along with two boiling chips. A Dean-Stark trap was then assembled, and 1.25 mL of hexane was added to the trap and marked with a pen. The value used was predetermined in the pre-lab by stoichiometric calculations. The Dean-Star trap was attached to the flask and condenser, and was heated on an aluminum block until the flask started to reflux. As the contents were heated, the solution turned from a peach color to purplish red. In order to prevent loss…

    • 1266 Words
    • 6 Pages
    Powerful Essays
  • Good Essays

    First, .26mL of 2.0mmol methyl Salicylate was measured and put into a reaction vial along with 2.5mL of 6M NaOH and a stir bar. The sample became a cloudy white color. The reaction vial was then connected to a reflux heating set-up and allowed to boil for twenty minutes until the cloudy white color dissolved into a clear liquid and then was allowed to cool. The sample was then transferred to a medium size beaker and slightly less than 2.5mL of sulfuric acid was added to the sample to adjust to pH 2. It was then placed in an ice bath to promote crystallization and then vacuum filtered to produce a white solid. The Salicylic Acid was the purified by adding 3mL of boiling water and then re-crystallization by placing it in an ice bath and vacuum filtering it. The sample was allowed to dry for a few minutes and then weighed. The weight was found to be .10g. The sample was then divided into two equal portions and one portion was mixed with the given sample of Salicylic Acid (made from benzene). Both samples where then tested in capillary tubes to calculate the melting point. The result of this step is represented in the chart below:…

    • 584 Words
    • 3 Pages
    Good Essays
  • Powerful Essays

    3 Darrell D. Ebbing , Steven D. Gammon, General Chemistry, 9th ed., Houghton Mifflin, Boston, 2009, p. 426.…

    • 1572 Words
    • 7 Pages
    Powerful Essays
  • Better Essays

    References: Darrell D. Ebbing and Steven D Gammon, General Chemistry, 9th ed. Cengage Learning: Ohio, 2009.…

    • 1680 Words
    • 7 Pages
    Better Essays
  • Satisfactory Essays

    The mere objective and purpose of this experiment is to use an esterification reaction in order to synthesize isopentyl acetate. This esterification reaction is between acetic acid and isopentyl alcohol and the catalyst we are using is concentrated sulfuric acid.…

    • 222 Words
    • 1 Page
    Satisfactory Essays
  • Good Essays

    Enzyme Reaction Lab

    • 868 Words
    • 4 Pages

    5. In beaker 2 (10 seconds) add the 10 mL’s of H2O2. Next add 10 mL’s of catalase. At the same time, press start on the timer. After 10 seconds add the sulfuric acid, to stop the reaction. Repeat step 3 and 4.…

    • 868 Words
    • 4 Pages
    Good Essays
  • Good Essays

    © Harcourt Education Ltd 2004 Salters Advanced Chemistry These pages have been downloaded from www.heinemann.co.uk/science…

    • 2823 Words
    • 12 Pages
    Good Essays
  • Satisfactory Essays

    Obtain an ice bath. 12 ml of concentrated sulfuric acid was gathered, cooled to 0 degrees Celsius, and put in a 125-ml Erlenmeyer flash. Then 6.1g of methyl benzoate was added. Then cooled in an ice bath to 0-10 degrees Celsius. A Pasteur pipette was used to add a cooled mixture of 4-mL of concentrated sulfuric acid and 4-mL of concentrated nitric acid.…

    • 479 Words
    • 2 Pages
    Satisfactory Essays
  • Satisfactory Essays

    Beers law

    • 480 Words
    • 2 Pages

    3. Label four clean, dry, test tubes 1–4. Use pipets to prepare five standard solutions according to the chart below. Thoroughly mix each solution with a stirring rod. Clean and dry the stirring rod between uses.…

    • 480 Words
    • 2 Pages
    Satisfactory Essays
  • Good Essays

    SCIN 131 Lab 02 Assignment

    • 1439 Words
    • 4 Pages

    References: SCIN131 Introduction to Chemistry Lab, November 2014, Section K001. (n.d.). Retrieved November 19, 2014, from http://my.thinkwell.com/students/index.cfm…

    • 1439 Words
    • 4 Pages
    Good Essays
  • Good Essays

    Bibliography: Burk, R. C., Azad, M., Sun, X., & Wolff, P. A. (2013). Introduction chemistry laboratory manual. (CHEM 1001/1002 ed., pp. 57-59). Ottawa: Carleton University.…

    • 1141 Words
    • 5 Pages
    Good Essays