Preview

Ap Chem Lab Report

Good Essays
Open Document
Open Document
1831 Words
Grammar
Grammar
Plagiarism
Plagiarism
Writing
Writing
Score
Score
Ap Chem Lab Report
Analysis of Alum
The objective of this lab is to run tests on a compound and analyze the substance itself, and then determine whether or not the compound is actually alum.

Jill Cline
Period 3
November 19, 2013
Laurel Hergenroeder and Sarinah Martelli
Introduction/Purpose
The purpose of this experiment is to run various tests on the substance called alum. (AlK(SO4)2 ∙ 12H2O). These tests like the process of filtration heating the solution will reveal things such as melting point, percent hydrate, as well as percent sulfate. After the experiment, the experimental mole ratio of alum to water will be calculated and then compared with the accepted mole ratio. (This is 12 to 1).
Theory
If this lab if conducted properly, the unknown substance will be determined to be alum because of melting point, percent hydration and percent sulfate. The first test that will be run has the purpose of revealing the alum’s melting point. Melting is defined as, the temperature at which a solid turns into a liquid. The melting point will help determine if the substance is an alum if its melting point is around 92.5° because this is the accepted melting point of an alum.
Then, the water will be evaporated from the substance, which will make it possible to find the percent hydration of the alum. A hydrate is a compound containing water: a chemical compound containing water molecules that can usually be expelled by heating. Anhydrous also will be a part of this lab because an anhydrous means to be with no water: describes compounds that contain no water, or crystals that lack chemically bound water of crystallization. The water will be expelled from the substance and begins hydrated but is then anhydrous because it will have no water in the end. Since the mass of the alum will be recorded before as well as after the water is evaporated, the two measurements will simply be divided (the larger as the denominator), yielding the percent hydration.

You May Also Find These Documents Helpful

  • Good Essays

    CHEM 1252 Lab Report 5

    • 1825 Words
    • 21 Pages

    The purpose of this experiment was to determine the differential rate law for a chemical reaction based on the relationship between the concentration of reactants and the rate of reaction. Since spectrophotometers, like Spec-20s, provide information about concentration, these instruments were used to monitor the increase or decrease in concentration of a reactant in a solution over time. By plotting [phph2-] versus time and changing the concentration of OH- used, the order of the reaction with respect to each reactant and the overall order of the reaction can be determined.…

    • 1825 Words
    • 21 Pages
    Good Essays
  • Satisfactory Essays

    The purpose of this lab was to learn how to determine the percent of water in a hydrate.…

    • 421 Words
    • 2 Pages
    Satisfactory Essays
  • Satisfactory Essays

    Chem 1211K Lab Report

    • 1855 Words
    • 18 Pages

    The identification of the melting point of the organic acid was done to find another characteristic of the acid and to test the purity of the recrystallized pure acid. A 2-4 mm layer of unknown sample was placed into a capillary tube sealed on one end. Then the capillary tube was inserted into the side a Bibby Sterlin device. The plateau was set to 200°C on the melting point apparatus. Once the plateau temperature was reached, the sample was watched carefully. When the sample first began to melt and when it was fully melted was recorded. These numbers were the range of the melting point. A slow melting point of the unknown organic acid and a standard sample was completed next. A new plateau was set about 10°C lower than the observed melting point of the unknown sample. This time once the plateau was reached, the heating was no more than 1°C per minute. This gave a much more accurate read of both melting points. If the standard did not melt in the range listed on the label of the bottle, that meant the machine was not working properly. The standard sample and the unknown organic acid melted in their appropriate ranges.…

    • 1855 Words
    • 18 Pages
    Satisfactory Essays
  • Satisfactory Essays

    Chemistry 116 lab review

    • 289 Words
    • 2 Pages

    The first step is to calibrate the colorimeter with0.20 M Fe(NO3)3and set the absorbance at 470 nm since it is known to keep an acidic solution throughout the entirety of the experiment. It was important to do this right at the beginning of the lab since the zeroed value of the acid was the calibration number for all of the other solutions. A total of seven solutions with different dilutions were used throughout the lab to conduct the equilibrium constant. The first step was adding 5 mL of 0.200 M Fe(NO3)3to each of the 5 test tubes. Once this was done, 0.00200 M NCS was added to the test tubes, each receiving a different amount; test tube one received 1 mL NCS-and with each test tube the amount of NCS-would increase by 1 mL, test tube 5 received 5 mL of NCS. . The next step was adding HNO3 to each test tube in different volumes; Test tube one received 10 mL of HNO3 and with each test tube the amount of HNO3 decreased by 1 mL, test tube five had no HNO3 added to it. The addition of these solutions formed five test tubes of different dilutions, but of equal volume, 10 mL each. After all of the previous trials had been completed the final step was to take each test tube and pour it into a different cuvette and measure the absorbance for each. Once the initial concentration was calculated of Fe3+, NCS and FeNCS2+ in molarity. The absorbency values were recorded and used to calculate the formation constant, K f The reference table containing volumes used in each solution is provided below…

    • 289 Words
    • 2 Pages
    Satisfactory Essays
  • Good Essays

    Ap Chemistry Lab Report

    • 678 Words
    • 3 Pages

    A 125 mL flask was obtained. The square of aluminum was fashioned over the flask by laying the foil over the mouth and folding the sides down. A pin was then obtained and was used to poke a tiny hole in the center of the aluminum cap.…

    • 678 Words
    • 3 Pages
    Good Essays
  • Good Essays

    Lab for Chemistry 221

    • 612 Words
    • 3 Pages

    Abstract: A 50mL (we used 100mL) volumetric flask was used to determine the amount of sugar in a can of Coke per mL in 5 different solutions. Using the calibration curve we determine the amount of sugar per mL in a can of coke. This experiment concluded that there is 43.83g of sugar in a 12oz can of Coke.…

    • 612 Words
    • 3 Pages
    Good Essays
  • Powerful Essays

    e. Research Problem: Is what we have alum? In this lab, we will be analyzing alum by doing three different tests. The first will be to find the melting point, the second to find the amount of water in alum, and the third is to find the percent sulfate. We expect the values to be close to the actual.…

    • 1909 Words
    • 8 Pages
    Powerful Essays
  • Good Essays

    Mole Formula Lab

    • 723 Words
    • 3 Pages

    The objective of this lab was to conduct an experiment to analyze the molar components in alum. This was conducted by heating the alum till the water had evaporated and then determining the number of moles for each component. Then using the these amounts to figure out the empirical formula for alum.…

    • 723 Words
    • 3 Pages
    Good Essays
  • Satisfactory Essays

    Quiz010: Lab Report

    • 929 Words
    • 4 Pages

    | LabRepQuiz010 Question MC #7: Which of the following is the best written sentence that includes the information below taken from an article written by Dr. Costanza, but avoids plagiarism?…

    • 929 Words
    • 4 Pages
    Satisfactory Essays
  • Good Essays

    No although there were no set questions listed before we started our experiment three hypotheses were developed one for each procedure. In the following three procedures there will be three separate amounts of Alum used all in different quantities. In procedure 1 the hypothesis was that if we melt 0.01g of Alum grinded into a powder, that it would be fairly similar to the literature temperature of 92 .5 degrees Celsius, and his hypothesis was based on the ideal knowledge that anytime you have 0.01g of Alum it would have the same or similar melting point. In procedure two the hypothesis was that if we took 2.00g of Alum crystals and heated it in a covered Crucible to drive off any water that the mass anhydrous Alum would decrease, this hypothesis was developed with the idea that all things contain H2O and if we eliminate that H2O and its mass that, the anhydrous substance itself would decrease in mass. Finally in procedure three hypothesis was that if we take 1.00g of Alum and mixed it with 50mL of distilled water, and 40mL of Barium Nitrate inside a beaker that the alone would mix with the Liquid, this is based on the basic science and definition of a solution where there is a solute and a solvent and take the mass of what would become Barium Sulfate. From there we would have to filter the new solution, see how much of…

    • 471 Words
    • 2 Pages
    Good Essays
  • Satisfactory Essays

    Lab Report #1 Che 101

    • 752 Words
    • 4 Pages

    While performing the lab experiments in the first unit, my observation included finding the appropriate tools in the kit in order to carry out the tasks. These experiments really showed me how to differentiate the types of tools we are using and understand the differences and reason for the differences in each. Touch was a big activated sense in these experiments, the heat from boiling the water and the cold ice from the temperature labs allowed for the connection between the results and the way the temperature felt.…

    • 752 Words
    • 4 Pages
    Satisfactory Essays
  • Better Essays

    There are twelve key principles of green chemistry that are used to evaluate how green a reaction may be. A green reaction prevents waste before it is created with little to no toxicity. Green experiments should be designed to maximize the starting materials into the final products while minimizing toxicity. Raw materials should be renewable and products should break down and not persist in the environment while reducing derivatives. All experiments should be performed in real time with use of catalysts while minimizing potential chemical accidents.…

    • 1312 Words
    • 5 Pages
    Better Essays
  • Powerful Essays

    Chem Lab Report

    • 1164 Words
    • 5 Pages

    .2400 grams of the unknown compound. This is done in duplicate and purple-tinted precipitates are placed in Gooch crucibles. The precipitates are suction dried using ethyl alcohol then acetone to…

    • 1164 Words
    • 5 Pages
    Powerful Essays
  • Good Essays

    Organic Lab

    • 3321 Words
    • 14 Pages

    1. What two effects do impurities have on the melting point of an organic compound?…

    • 3321 Words
    • 14 Pages
    Good Essays
  • Good Essays

    Hydrate Lab

    • 434 Words
    • 2 Pages

    The mass of the anhydrous salt depends on the mass of the hydrate because the crystal lattice is a fixed ratio of the salt and water. This experiment essentially proved that by heating a crystal which contains water in its lattice structure, water can be extracted resulting in only the salt in a changed color. Our salt changed from blue to white upon heating it. Since our laboratory is not under perfect conditions, there are several sources of error. Human errors included incorrectly registering the mass of the salt or accumulation of left over…

    • 434 Words
    • 2 Pages
    Good Essays